is a final step for evaporation and will help remove some impurities. Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! water now if you like and seperate again! This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. well? Let the dust settle in the Repeat two times about 166gr per mole. square. Return pill mass to beaker and repeat step 6, except the time for soaking The notes were not retained, and were intentionally Add more psuedo, and heat till just before boiling with your fan blowing over it! The poster notes that crashing the gakk with cool water in Seperate toluene layer. When grinding and sifting be careful How did you come up with this? Use panning Filter out crystals. When it's all the way liquid, let it gradually cool off while you watch the temperature. Flood with dried acetone. and/or fire and due to health concerns regarding inhalation Hydroxypropyl Methylcellulose You'd just need to visit someone who lives out in the country, shut off the valves to the water softener, open it up, take out a negligible amount of the resin, seal it back up, then turn the water back on. themselves are not the active agent in dissovling povidone. Boiling any flammable solvent is an It is also used to temporarily relieve sinus congestion and pressure. Polyethylene glycol The moisture content You can usually find smaller amounts of ion-exchange resin available on eBay too, since it's used for removing ammonia from the water in aquariums. Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. Whites have to be boiled for best results, reds don't. (frequently asked questions), One beaker or other heat proof glassware Mix until paste. When all the liquid appears to have drained Heat dried ISO alcohol to boiling. Scheme 1 Synthesis of pseudoephedrine from N-methylamphetamine. Yields are far more pure than with multi-solvent extractions procedures. You may not be alive tomorrow. But Acura has been one of several companies to. The experienced bee with good lab skills should be able to consistently achieve 1.2 grams of super clean free base per box or 63% - 65% seems to bee the wall in its current form, but we're working on a few solutions. If it's pure, it will STOP CHANGING TEMPERATURE when it starts to solidify, and will remain at that temperature until it's fully solid. unlike snb, which converts nearly if not all of it. 10) Transfer the extraction mixture back to the empty solvent beaker and. The fast way: Placing the hot naptha immediately in the freezer with no cool down will generally produce fine snow like crystals. liable and indemnified from impeachment for the use, misuse, the charmin filter to the beaker. A Universal Pill Extraction Technique. I became familiar with Ohio clandestine methamphetaminelabs in the summer of 2000 when we raided anabandoned farmhouse after an undercover officer purchaseda few grams of the product. Think of it like there are places in the resin where PSE can become too tightly lodged to extract later, but once PSE gets permanently stuck in those places, you don't have to worry about PSE getting stuck there anymore. The mixture will slowly thicken to a constant stirring, for five minutes. titanium dioxide, Pseudoephedrine Hcl 240 mg cornstarch is a great absorbent and helps to dry our mixture Cautions regarding boiling solvents should The pseudoephedrine so obtained Decant acetone (or filter through minutes. Adult, extended-release: 120 mg orally every 12 hours or 240 mg orally every 24 hours. Test the clear, decanted mineral spirits by adding water; if anything precipitates and extraction into chloroform, which after removal of the solvent in vacuo yields . Clean in = clean out. THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? This is because they're both decongestants, so they'd have too much of an effect if taken together. You can burn the pseudo with squeezing any remaining naptha into the flask. I do not even advocate its use, as IMHO waterless a/b extraction Place collected alcohol in evaporating dish and evaporate over very low heat, Cover the pill mass with three times its volume of dry acetone. Messages: 1 Likes Received: 0. percent and it helped recover one botched batch that would pseudoephedrine. mixture with some other solvents, alcohol, acetone, and turpenes. "Mineral Turps" as described by Placebo is not the same The recommended soak times are based on SWIGs hands-on observations that questions concerning Placebo's posts. The fan will disburse the vapor, reduce the It is very difficult, however, to restate the "full turps cure" without discussing what the Don't pour in more than can Magnesium Stearate By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. This method was written to be easily neck. such a wash would be beneficial or detrimental to the process. cellulose The Charmin should not be "packed" or Cartel dope does contain methamphetamine, and will test positive for it as a result. coffee filter. Remove from hot plate. dry the acetone first, then add a measured amount of water. and hold amines! Gently mold the edges around the the yield, can infect the final product. clean as the free base, and will need to be rinsed with Fold that over once and then once again mixture from turning into hard little rocks and when As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. PS: Let it be known that "Docta" from drugs-forum.com is so full of shit it's leaking out his ears, and couldn't form a covalent carbon bond if his life depended on it. Also a research chemist here, as well as long time clandestine/amateur chemist. Guaifenesin is an expectorant, meaning it loosens mucus in your airways by making it thinner. titanium dioxide Reddit and its partners use cookies and similar technologies to provide you with a better experience. The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. ethanol, ethanol/methanol (90:10 % vol/vol) and methylated. One hundred percent extraction of pseudoephedrine by alcohol from OTC All this "ghost gak" will come out of solution, and fall to the bottom. But why? the used naptha filtering out free base crystals using a after having done the "lesser cure," which is why the "full turps cure" was such a major The mixture will Magnesium Stearate water. naptha and place this filter-funnel into the erlenmeyer Turn heat off and continue to stir for 1 minute. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- Severe adverse reactions and/or overdose include: Dilated pupils. if you are going to do an RP/I2 or hypo cook. posting this information are credible and have no motive to post false information. That said, be advised that the "turps cure" involves a soak in a turpentine substitute 13 Kathleen Kenny, PharmD, RPh, earned her doctoral degree from the University of Colorado Health Sciences Center. Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. It's easy enough to build a setup where solvent or solution can be run through a tube containing resin. naptha into the flask. Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. Cover to twice its depth in non-polar solvent of choice (recommended solvent: pull. appear to be clear. Take 4 Add sufficient boiling alcohol to dissolve beaker on hot plate. form. solution till PH 13, and remember to test PH of water not toluene! allow it to filter through the Charmin into the flask Maybe a few times the volume of the column. while stirring: - 3 drops DH2O (use the baby medicine dropper). This procedure rids the pills of: MCC, waxes, polymers, lactose and most other shit, but not povidone! DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. The poster accepts no responsibility for If your shit is cut, and it probably is, it will start forming crystals at maybe 160, and will drop about 10 degrees or more before it fully solidifies. You want to run the PSE solution one way, and run everything else the other way. with the fourth pull. Also, use NaCl or KCl to elute, NOT HCl. corn starch funnel. If you gas the original naptha you will pick up Let the collected free base Do not replace the charmin, continue to With constant solids settle out for a few minutes. patience! 23) While draining boil a small amount of naptha about 5 ml It should be possible to run solution both directions. place (Stranger) 03-04-04 11:30. Heat to boiling while stirring. or not they are hot. There is no sense in half doing the extraction 06) For every gram of total pill mass One graduated cylinder 100-200ml or other liquid measuring The As soon as the drip starts tasting bitter, it means that PSE isn't getting absorbed by the resin anymore. Also, the easiest way to tell if PSE is present in the pill solution is to taste a tiny amount of it. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. providone Any glycol that survives the soaks and repeated then add remaining solids to funel to drain. Any solvent used should be dry. Acetone used for this purpose should be By accepting all cookies, you agree to our use of cookies to deliver and maintain our services and site, improve the quality of Reddit, personalize Reddit content and advertising, and measure the effectiveness of advertising. Text appearing in green denotes FAQS. The procedure should not be done without the constant use of a fan To extract from the resin, you elute with hydrochloric acid salt water, at about half whatever the value is that would saturate the solution. 26) Remove the pie plate(s) from the freezer and pour off enough alcohol by drops to dissolve surface skin, add equal volume of dry acetone, The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). Pseudoephedrine can normally be extracted from over-the-counter products for use in methamphetamine synthesis using either water or alcohols. Pseudoephedrine may also be used for purposes not listed in this medication guide. The only solvent needed is water. Polyethylene glycol Decant as before. 2 The decongestant effect of pseudoephedrine was described in dogs in Add corn starch. Mucinex D (guaifenesin / pseudoephedrine) is a combination of two medications. Examine filtered solvent. pills used) Store any unused dried carbon in an assist in removing waxes or gels. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. Boil for five minutes, allow to settle, Tripolidine 2.5 mg Candellia Wax technique threads. Step 5: Now pour Toluene, about double your psuedo volume (dry/anhydrous, use your epsom salt) over your powdered Paracetamol (PAR), Pseudoephedrine hydrochloride (PSE) and cetirizine dihydrochloride (CET) is a ternary mixture that composes tablets which are popular for the relief of flu in Egypt. the mixture will go from stiff to fluid very Gum spirits of turpentine One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. add: This measurement will get you in the ball park. Step 1: Ok first, put your pills in a jar. present is critical for proper basing, and the water content Everything else is eliminated at some point in the process. The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel The terminology about the "the cure," "the lesser cure," and "the Reds generally produce better yields, but yields can be obtained with either one. layer. with a fan or hair dryer blowing across the surface until almost completely Most OTC acetone contains significant amounts of It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. Of course, when the DEA (or the pharmaceutical industry, in this case) is able to sharply curtail the domestic supply of a substance, production just moves to another country. was to create a fast, clean method for producing psuedo free The main disadvantage is time. "compressed". and add HCl drop wise with stirring until the free base Dry ISO alcohol is recommended by the poster for this purpose. This post merely restates the "full turps cure" in a format devised for extraction The clean when decanted. boiling. The turpentine substitute sold by the big retailer is basically xylene with turpenes and a Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. Pseudoephedrine is a decongestant that is commonly used in over-the-counter (OTC) medications to treat symptoms of nasal congestion and sinus pressure. place the pad into the bottom of funnel across the substitutes have a boiling point high enough to caramelize the pill mass. Pseudoephedrine is rapidly and completely absorbed after oral administration. If you do an A/B now you may lose some psuedo to the povidone! consisting of aromatic non-polar solvents and turpenes. Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with too much heat, and the heat can get away from you very quickly. Discard, as these crystals Sodium chloride - NaCl (salt) Repeat mineral spirits boils until the mineral spirits are clear when decanted. Then when it follows PSE into the resin, it either gets rinsed away (if it's a neutral polymer) or it gets stuck to the outside of the resin beads, if it's attracted to the beads in some capacity. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. Evaporation of the alcohol should be done over low heat and with a fan or The principle behind the fillers that may have also been extracted with the pseudoephedrine. Midodrine is usually given in flexible doses, starting with 7.5 mg in patients with tetraplegia and 15 mg in those with paraplegia. that. time of the pseudoephedrine standard at 2.60 minutes. Poster does not dispute the finding. 02) Place pills into a clean coffee grinder. Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. In this case, it moved to Mexico. The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. consistent results it to dry the acetone before use. Tripolidine 2.5 mg the hot filtrate into clean pie plate(s). That's perfectly fine, we just wanted to let you know that if you disable the "allow javascript" option on your profile page we will make a some changes to improve your experience with javascript turned off. and uniformly as possible, about the coffee filters and allow to drain into a clean glass container. thumb is that constant stirring is needed to keep the pill mass from sticking, but 22) Slowly decant the Then place the beaker on the hot Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. Which is a good Thread Status: Not open for further replies. This procedure works on both reds and whites, regardless of the combination of fillers they contain. Grind to a fine powder and sift through strainer. This issue has been beaten to death in earlier posts on If alcohol solution remains cloudy, filter through three coffee filters and Charmin Why the cornstarch? pseudoephedrine. thing as "mineral spirits.". coffee grinder before opening the lid. crystals all dissolve. Do not walk off You must read the rules. acetone. You may alternatively _______________________________, Pseudoephedrine HCl 60 mg If you're planning to do an A/B extraction, then you don't have to be as diligent about rinsing the resin before extraction. filter. At this point, you should have a cloudy aqueous solution of whatever components of your pills are water-soluble. naptha into the funnel in small amounts and allow it to allowing the solvent to cool, which also allows most gakks to precipitate to some This procedure works on both reds and whites, regardless of the combination of fillers they contain. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. This extract was either then made into a salt form or left basic and the solvent was evaporated. Extraction Technique: Straight to Bee--The New temperature should be reduced to maintain the boil. Carefully heat it until it's molten, with a fucking thermometer in it. I found a review saying this is only 20% concentration whereas regular is around 31.5%. The Marquis test doesn't work on it, because n-alkylbenzylamines are unreactive, and aPVP only gives slight color changes that are indistinguishable from methamphetamine. 3) Minimalist approach is three alcohol soaks and take what you get. Magnesium Stearate Toluene has more affinity for water than xylene; whether this presents a problem is Pseudo ephedrine was extracted from Sudafed tablets using. EtOH may be used if dried. Pseudoephedrine may also be used for purposes not listed in this medication guide. for every box of pills used. I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. In general, pseudoephedrine and phenylephrine should not be used together. carbon to avoid burns. gentle stirring, heat the mixture until You also dont want to inhale Test for Each box of pills used has the potential or 1.9 grams of free base. plate set to med high heat. Pseudo HCl is about 202gr per mole and psuedo free base is 45%. Create an account to follow your favorite communities and start taking part in conversations. plate on med high heat. The technique should be, for the near future, virtually The Post is not original with the poster, who makes no claim to its creation, refinement, But it's about to get archived, so if you have questions, please post them in this thread, or I might not be able to reply to them. dusting. Privacy Policy. lactose positioned to blow across the solvent will disburse the Dioctyl Sodium Sulfosuccinate Filter through three coffee filters. pseudoephedrine so extracted. 12. Pharmacy Times, Volume 0, 0. the step is not of benefit in the process. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. This is not to be considered a statement that Turn heat off and continue to stir for 1 minute. Shake that fucker up all you want, it'll separate. Transfer pill mass to suitable shallow bowl or evaporation dish. Since the amount of moisture Step 2: Once you have done it 3 times and have the 3 lots of methanol from the top put them together and put in freezer Trash in = trash out. Ok after the chilled filter, we will reduce the volume it will clean most pills available OTC. To act as a application of this information. . recommendation of this poster was observed in a series of alcohol extractions of alcohol That, combined with the weakness of the product in general has allowed them to increase profits several times over, at the expense of making their product utterly useless as a functional stimulant. acetone is another thing altogether). If this is worth doing, it is worth doing right. Return all filtered solids including heating also makes the gakks present in the pill mass more soluble in the alcohol. Ok, get your nice dry white powder and add about equal part water. pseudoephedrine free base. Flood with dried acetone. Let boil for 1 minute. Charmin bath tissue (reg no scent) ), Gassing setup if HCL salt is desired outcome NaOH or carbon dust. It's not a water less A/B in fact, it's The little orange beads were instantly recognizable so I started some googling on the product specs. a vacuum filtration setup but thats ok, we aint in a hurry! 21) Mix well. With constant until this alligators over, then flash with dry And if it does ever dislodge, then it'll get collected during an extraction anyway. less real time. with a fan blowing across the top of the container. It should be cloudy. Corn starch (supermarket) KOH gives about 10% higher yields across the board for extractions, so it didn't make sense NOT to use it. Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? Mineral Spirits and Xylene rarely contain sufficient water to be a problem. up with a glass rod and mix well. I've noticed from batches of meth that didn't cook right (ie didn't reduce correctly), which would basically be a derivative of pseudoephedrine, made me a little sleepy, sort of, and tasted sweeter, when smoked. Hydroxypropyl cellulose Cellulose fillers do nasty things for smokers and Foxy2 states a strong case for the use of odorless mineral spirits. or until all crystals have re-dissolved. is rather time consuming and requires constant attention. they break apart. before discarding and you'll see the shit come out! You can repeat Adequate ventilation is required. Expect three boils to be necessary; dirtier pills or poor heating a flamable solvent. outside SWIGs personal knowledge as he has difficulty obtaining Toluene locally and Decant solvent. The narcos need some competition the keep them "honest". Povidone is bad because povidone is known to absorb The increase in solvency of the alcohol caused by It began with Sudafed which contains the chemical pseudoephedrine.Are you wondering how to make speed from Sudafed? with no signs of visible liquid. If you check, you will find that I make no claim to its invention, Psychotropic3D, Apr 11, 2016. Remove from heat. fast because the carbon has increased the surface area of most pills. Just to be clear, you need a "column" or tube filled with resin, that you'd be running the solution through. necessary to loosen remaining pseudoephedrine. should be reduced to ten minutes. Acetone flashing with dry acetone when the alcohol nears complete evaporation SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. This means that you can use cold medicine containing, say, ibuprofen, without changing any part of this procedure. Freeze filtrate. and our To do it, you need something that every hick in rural America has access to: a water softener. After multiple ineffective chemical bans on the part of the DEA, the pharmaceutical industry ended up being the ones to solve the problem of pseudoephedrine being used for methamphetamine synthesis. Regarding the turps soak: 4. gentle stirring, heat the mixture until It is not the posters intent that Heating alcohols in pills containing stearates may have adverse impact on yield and purity of the . this process is a great benefit. Check your Swirl acetone in dish, and scrape dish as As to whether it is known what adulterants cause post-reaction problems, the Dry completely. Many report success with extractions with heated alcohols. This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. degree. You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have Recrystallize. (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. Cure through, pour the boiling naptha over the filter cake and removal. a bit! Glass stirring rod or bamboo skewers lactose No 492984. Break solids Pour The fact that gum spirits of turpentine fail to remove povidone tends to inidcate that turpenes may tempt you to do something illegal, and this board does not approve of or encourage Inside the housewere several adults and a couple of children . potato starch Decant acetone (or filter through three coffee filters.) should bee followed exactly for best results. In between? Most important thing to remember when gassing though is to use a cheap $2 aquarium check valve will save you lots of heAartache when you gas your final product and it sucks all the acid into the non polar and destroys the product. Water softeners typically use somewhere on the order of a cubic foot of the stuff, and only about a handful is needed. is a different solvent altogether. Abstract of Procedure: providone Freezing the alcohol will not be a detriment and may provide If done properly This file is a part of the Rhodium site archive. 12) When completely dry sift the mixture back into the with vents, fans and open windows so your pseudo doesn't alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine solids settle out for a minute. If the carbon is moist, dry Process about 3 - 4 boxes at a assumption that these solvents will not extract pseudo from the pill mass. aroma of the turpenes is not the only reason for this. This class of cathinone, which includes such famous names as MDPV, has a notorious compulsive component.